Download Advances in Organic Chemistry, 50 (Advances in Inorganic by AG Sykes, Alan H. Cowley PDF

By AG Sykes, Alan H. Cowley

Advances in Inorganic Chemistry provides well timed and informative summaries of the present development in numerous topic parts inside of inorganic chemistry, starting from bioinorganic to good kingdom. This acclaimed serial beneficial properties studies written by way of specialists within the sector and is an crucial connection with complicated researchers. every one quantity of Advances in Inorganic Chemistry includes an index, and every bankruptcy is totally referenced.

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Hey-Hawkins et al, Chem. Commun. 1992, 775. Copyright 1992, the Royal Society of Chemistry. 46 KEITH IZOD (DME)]2 has also been reported and is structurally similar to 6 (44). , 6 and 7 may be regarded as two- and four-rung ladder species). In 6, 7, and 8 the Li and P ˚ . 05 A [Li(tmeda)2][P(SiH3)2] has also been structurally characterized (48). 194(6) A ˚ ]. 222(6) A Driess et al. have reported the synthesis and structures of two novel sterically hindered silicon-substituted lithium phosphides [Li͕P(SiPh3)2͖]2 (9) and [Li4͕PH(SiPr i3)͖͕P(SiPr i3)2͖3] (10) (49).

11. Dias, H. V. ; Jin, W. Tetrahedron Lett. 1994, 35, 1365. 12. ; Teles, J. ; Brode, S. Angew. , Int. Ed. Engl. 1995, 34, 1021; (b) Arduengo, A. , III; Goerlich, J. ; Marshall, W. J. Leibigs Annl Recl. 1997, 365; (c) Alder, R. ; Butts, C. ; Orpen, A. G. J. Am. Chem. Soc. 1998, 120, 11526. 13. Arduengo, A. , III; Gamper, S. ; Calabrese, J. ; Craig, H. A. J. Am. Chem. Soc. 1995, 117, 572. 14. Arduengo, A. , III; Dias, H. V. ; Calabrese, J. ; Davidson, F. Organometallics 1993, 12, 3405. 15. Herrmann, W.

Copyright 1997, Wiley-VCH. molysis gives the diphosphasilacyclopropane ͕(Is)2Si͖PHUP͕SiF(Is)2͖ (59). Reaction of this compound with BuLi in THF leads to the unusual lithium phosphide [͕(Is)2Si͖-P͕Li(THF)3͖-P͕SiF(Is)2͖], which has been structurally characterized by X-ray crystallography. Thermolysis of this complex yields the bicyclophosphasilane ͕(Is)2Si͖2P2 . The aminophosphine-functionalized lithium phosphide complexes [Li͕P[SiF(Is)2][P(NR2)2]͖(THF) (R ϭ Me, Pri) have also been reported to undergo novel thermally induced decomposition reactions (52).

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