Download Annual Reports in Inorganic and General Syntheses–1975 by Hans Zimmer PDF

By Hans Zimmer

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L4756lf. W. Min, DISS. ABSTR. INT. , 36,710 ( 1 9 7 5 ) : CHEM. , 179247z. R. Fish, E. Kimmel, J. Casida, J. ORGANOMET. , 91,C1 ( 1 9 7 5 ) . P. Van Leeuwen, R. Kaptein, R. Hüls, W. Kalisvaart, J. ORGANOMET. , 91,C5 ( 1 9 7 5 ) . P. Mazerolles and A. Paucher, J. ORGANOMET. , 85,159 (1975). V. Nikanorov, V. Rozenberg, R. Gorbacheva, Y. Bundel, and 0. Reutov, J. ORGANOMET. , 101,259 ( 1 9 7 5 ) . K. Bos, E. Bülten, J. Noltes, J. ORGANOMET. , 99,397 ( 1 9 7 5 ) . A. Nexmeyanov, T. Tolstaya, and V.

M e h r o t r a , G. S r i v a s t a v a , and R. M e h r o t r a , I N D I A N J. C H E M . , 1 3 . 1 6 3 (1975). D. D a t t a , B. M a j e e , and A. G h o s h , J. O R G A N O M E T . , 8 4 , 2 3 1 ( 1 9 7 5 ) . R. C r a g g , A. T a y l o r , J. O R G A N O M E T . , 9 9 , 3 9 1 (1975). I. H a l d u c , F. M a r t i n a s , D. R u s e , and M. C u r t u l , SYNTH. REACT. INORG. -ORG. , 5 , 1 0 3 (1975). Z. N o v i k o v a , S. M a s h o s h l n a and I. L u t s e n k o , ZH. O B S H C H . , 4 5 , 1 4 8 6 ( 1 9 7 5 ) : CHEM.

The products obtained from reaction of Si(SiCl3)4 with methanol depend on reaction conditions. If a molar deficiency of MeOH/Et20 is added at low tenperature followed by MeOH/Et3N/Et20, [ (MeO)3Si]2Si (97%) is obtained, however when the appropriate amount of MeOH/Et3N is added dropwise, the products are [(MeO)^Si]^SiH and [(MeO)^Si]2SiH2 (122). Silylperoxides are prepared from chlorosilanes and alkylhydroperoxides. From 1 to 4 peroxo groups may be incorporated but yields of product usually decrease with increasing numbers of peroxo groups (123,124,125, 126,127).

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